著者
Marc Schröder Kyoko Nozaki Tamejiro Hiyama
出版者
(社)日本化学会
雑誌
Bulletin of the Chemical Society of Japan (ISSN:00092673)
巻号頁・発行日
vol.77, no.10, pp.1931-1932, 2004 (Released:2004-10-09)
参考文献数
17
被引用文献数
21

Treatment of phosphine–boranes with molecular sieves 4Å in a mixture of an ethereal solvent and an alcohol provided deprotected free phosphines in quantitative yields. The phosphines can be obtained by a simple filtration/crystallization procedure in most cases. It should be noted that the current method is successfully applied to the deprotection of a phosphite–borane for the first time.