著者

山元 俊憲 寺田 賢 吉田 武美 吉村 三郎 黒岩 幸雄

出版者

公益社団法人日本薬学会

雑誌

衛生化学 (ISSN:0013273X)

巻号頁・発行日

vol.27, no.5, pp.326-330, 1981-10-31

被引用文献数

3

---

Sympathomimetic amines, amphetamine and methamphetamine, were determined as trifluoroacetyl derivatives by gas chromatography (GC) equipped with a flame-thermionic detector (FTD). Resolution of these derivatives was carried out in a glass column (3 mm×1 m), packed with 1.5% SE-30 on Chromosorb W (AW-DMCS) at 110℃, with helium at a flow rate 50 ml/min. Detection limit of these amines was 0.1 ng. In a case of the autopsy samples from 4.5 month-postmortem suspected the intoxication of methamphetamine, we could detect the amine by FTD-GC, and the content was calculated to be 12.5 μg per g wet weight liver.