- 著者
- Shunichi SUDA Akimasa TSUJIMOTO Wayne W. BARKMEIER Kie NOJIRI Yuko NAGURA Toshiki TAKAMIZAWA Mark A. LATTA Masashi MIYAZAKI
- 出版者
- The Japanese Society for Dental Materials and Devices
- 雑誌
- Dental Materials Journal (ISSN:02874547)
- 巻号頁・発行日
- pp.2017-059, (Released:2017-11-23)
- 参考文献数
- 51
- 被引用文献数
- 20
The effect of phosphoric acid pre-etching on enamel bond fatigue durability of universal adhesives and two-step self-etch adhesives was investigated. Four universal adhesives and three two-step self-etch adhesives were used. The initial shear bond strengths and shear fatigue strengths to enamel with and without phosphoric acid pre-etching using the adhesives were determined. SEM observations were also conducted. Phosphoric acid pre-etching of enamel was found to increase the bond fatigue durability of universal adhesives, but its effect on two-step self-etch adhesives was material-dependent. In addition, some universal adhesives with phosphoric acid preetching showed similar bond fatigue durability to the two-step self-etch adhesives, although the bond fatigue durability of universal adhesives in self-etch mode was lower than that of the two-step self-etch adhesives. Phosphoric acid pre-etching enhances enamel bond fatigue durability of universal adhesives, but the effect of phosphoric acid pre-etching on the bond fatigue durability of two-step self-etch adhesives was material-dependent.
- 著者
- Kazutaka HIRAI Akimasa TSUJIMOTO Kie NOJIRI Hirofumi UETA Toshiki TAKAMIZAWA Wayne W. BARKMEIER Mark A. LATTA Masashi MIYAZAKI
- 出版者
- 日本歯科理工学会
- 雑誌
- Dental Materials Journal (ISSN:02874547)
- 巻号頁・発行日
- pp.2016-019, (Released:2017-06-23)
- 参考文献数
- 31
- 被引用文献数
- 4
The influence of photoirradiation conditions on dentin bond durability and interfacial characteristics of universal adhesives was investigated. Universal adhesives were applied to the dentin surfaces and photoirradiated with 100 mW/cm2 for 40 s, 200 mW/cm2 for 20 s, and 400 mW/cm2 for 10 s. A resin composite was bonded to dentin to determine shear bond strength after 24 h water storage and 30,000 thermal cycles, and water contact angle of cured adhesive were measured by the sessile drop method. Greater dentin bond strengths after 24 h water storage and 30,000 thermal cycles were achieved under these conditions at light intensity exceeding 200 mW/cm2. Universal adhesives photoirradiated above 200 mW/cm2 exhibited significantly higher water contact angles than those at 100 mW/cm2. The results of this study suggested that the photoirradiation conditions affect the dentin bond durability and interfacial characteristics of universal adhesives even at the same total energy.
- 著者
- Fumi YOSHIDA Akimasa TSUJIMOTO Ryo ISHII Kie NOJIRI Toshiki TAKAMIZAWA Masashi MIYAZAKI Mark A. LATTA
- 出版者
- 日本歯科理工学会
- 雑誌
- Dental Materials Journal (ISSN:02874547)
- 巻号頁・発行日
- vol.34, no.6, pp.855-862, 2015-11-27 (Released:2015-12-01)
- 参考文献数
- 28
- 被引用文献数
- 2 37
This study investigates the influence of surface treatment of contaminated lithium disilicate and leucite glass ceramic restorations on the bonding efficacy of universal adhesives. Lithium disilicate and leucite glass ceramics were contaminated with saliva, and then cleaned using distilled water (SC), or 37% phosphoric acid (TE), or hydrofluoric acid (CE). Specimens without contamination served as controls. The surface free energy was determined by measuring the contact angles formed when the three test liquids were placed on the specimens. Bond strengths of the universal adhesives were also measured. Saliva contamination and surface treatment of ceramic surfaces significantly influenced the surface free energy. The bond strengths of universal adhesives were also affected by surface treatment and the choice of adhesive materials. Our data suggest that saliva contamination of lithum disilicate and leucite glass ceramics significantly impaired the bonding of the universal adhesives, and reduced the surface free energy of the ceramics.
- 著者
- Kie NOJIRI Akimasa TSUJIMOTO Takayuki SUZUKI Syo SHIBASAKI Saki MATSUYOSHI Toshiki TAKAMIZAWA Masashi MIYAZAKI
- 出版者
- 日本歯科理工学会
- 雑誌
- Dental Materials Journal (ISSN:02874547)
- 巻号頁・発行日
- vol.34, no.5, pp.611-617, 2015-10-02 (Released:2015-10-05)
- 参考文献数
- 28
- 被引用文献数
- 5 8
In this study, we investigated the influence of light intensity on the surface-free energy and dentin bond strength of single-step selfetch adhesives. The adhesives were applied to the dentin surfaces of bovine mandibular incisors and cured with light intensities of 0 (no irradiation), 200, 400, and 600 mW/cm2. Surface-free energies were determined by measuring the contact angles of three test liquids placed on the cured adhesives. Dentin bond strengths of the specimens were also measured. Polymerization with a higher light intensity resulted in a lower surface-free energy of the cured adhesives. The greatest bond strength was achieved when a light intensity of 400 mW/cm2 or greater was used. Our data suggest that the surface-free energy and dentin bond strength of single-step self-etch adhesives are affected by light intensity of the curing unit.