著者
松岡 三郎 古谷 佳之 竹内 悦男 蛭川 寿 松永 久生
出版者
一般社団法人 日本機械学会
雑誌
日本機械学会論文集 (ISSN:21879761)
巻号頁・発行日
vol.87, no.895, pp.20-00439, 2021 (Released:2021-03-25)
参考文献数
16

In order to clarify the effect of internal hydrogen on the fatigue life properties of SUS304, SUS316 and SUS316L, tensile tests and low- and high-cycle fatigue life tests were carried out in air at room temperature using 10, 68 and 100 MPa hydrogen-charged specimens. High-cycle fatigue life tests demonstrated that S-N curve (i.e., relationship between stress amplitude, σa, and number of cycles to failure, Nf) of each steel was higher in hydrogen-charged specimen than in uncharged specimen. The increase in fatigue limit, Δσw, with internal hydrogen was 40 MPa in 100 MPa hydrogen-charged specimens, 20 or 30 MPa in 68 MPa hydrogen-charged specimens, and 0 or 10 MPa in 10 MPa hydrogen-charged specimens. Low-cycle fatigue life tests manifested that εta-Nf curve (i.e., relationship between total strain amplitude, εta, and number of cycles to failure, Nf) of 68 MPa hydrogen-charged specimen was nearly coincident with that of uncharged specimen in SUS316L, whereas 68 MPa hydrogen-charging markedly lowered εta-Nf curve in SUS304. The fraction of strain-induced martensite was measured on specimens fractured by tensile tests and low- and high-cycle fatigue life tests. The critical value of the martensite fraction below which 68~100 MPa hydrogen-charging does not cause hydrogen embrittlement, fmH, was 1 % in tensile tests. On the other hand, the fmH value was 9% in low- and high-cycle fatigue life tests. The increase in fatigue limit due hydrogen-induced solid solution strengthening, Δσw, in high-cycle fatigue life tests was expressed as Δσw (MPa) = 15.4 × 237H, where H is the hydrogen content (mass %). In addition, the hydrogen-induced strengthening of stress amplitude, Δσa, and 0.2% proof strength, Δσ0.2, in low-cycle fatigue life tests was expressed as Δσa+0.2 (MPa) = 15.4 × 296H. The results inferred that the contribution of hydrogen to solid solution strengthening was about 10 times larger than that of carbon and nitrogen when compared at the same mass concentration.
著者
松岡 三郎 松永 久生 山辺 純一郎 濱田 繁 飯島 高志
出版者
一般社団法人 日本機械学会
雑誌
日本機械学会論文集 (ISSN:21879761)
巻号頁・発行日
vol.83, no.854, pp.17-00264-17-00264, 2017 (Released:2017-10-25)
参考文献数
29
被引用文献数
19

Considering in design by analysis, four types of tests, slow-strain-rate tensile (SSRT), fatigue life, fatigue crack-growth (FCG), and elasto-plastic fracture toughness (JIC) tests, were conducted with low-alloy steels, JIS-SCM435 and JIS-SNCM439, in 115 MPa hydrogen gas and air at room temperature (RT). In addition to above tests at RT, the SSRT tests were also conducted in 115 MPa hydrogen gas and air at 120 oC and in 106 MPa hydrogen gas and 0.1 MPa nitrogen gas at -45 oC. The low-alloy steels used in this study had tensile strengths (σB) ranging from 824 to 1201 MPa with fine and coarse tempered-martensitic microstructures. In the SSRT and fatigue life tests, the tensile strength and fatigue limit were not degraded in hydrogen gas. The FCG tests revealed that the FCG rate (da/dN) was accelerated in hydrogen gas; however, there existed an upper bound of the FCG acceleration, showing the FCG rate in hydrogen gas was about 30 times larger than that in air, when σB was lower than 900 MPa. The JIC tests demonstrated that the fracture toughness (KIC) in air was 207 MPa·m1/2 at σB = 900 MPa, whereas the hydrogen-induced crack-growth threshold (KI,H) was 57 MPa·m1/2 at σB = 900 MPa. Based on these results, we proposed advanced guidelines on the use and design for SCM435 and SNCM439 on design by analysis in 115 MPa hydrogen gas, which enable to design the storage cylinders used in 70 MPa hydrogen station with lower cost without compromising safety.
著者
松岡 三郎
出版者
明治大学法律研究所
雑誌
法律論叢 (ISSN:03895947)
巻号頁・発行日
vol.78, no.2, pp.125-169, 2006-01
著者
宮原 健介 松岡 三郎 長島 伸夫 三島 周三
出版者
一般社団法人日本機械学会
雑誌
日本機械学會論文集. A編 (ISSN:03875008)
巻号頁・発行日
vol.61, no.590, pp.2321-2328, 1995-10-25
被引用文献数
13 12

A nanoindentation hardness apparatus was developed on the basis of an atomic force microscope to obtain both an indentation curve and an indentation image. Newly devised features were to use a lever which has a three-sided pyramidal diamond tip at the central part of the lever, to measure the vertical displacement at the center of the lever and to add an actuator for controlling the force. The ultra-microhardness values of gold, SUS403 steel and SNCM439 steel measured at the indentation forces between 2.6×10^3 and 3.5×10^3 μN using the nanoindentation hardness apparatus agreed with the macrohardness values measured at the force of 4.9 or 9.8 N using the conventional Vickers hardness apparatus. However, the ultra-microhardness increased with decreasing indentation force. This behavior was explained considering the elastic-plastic conditions of the specimens.
著者
金崎 俊彦 楢崎 千尋 峯 洋二 松岡 三郎 村上 敬宜
出版者
一般社団法人日本機械学会
雑誌
日本機械学會論文集. A編 (ISSN:03875008)
巻号頁・発行日
vol.72, no.723, pp.1717-1724, 2006-11-25
被引用文献数
11 17

The effect of hydrogen on fatigue crack growth behavior of four stainless steels has been investigated from the viewpoint of martensitic transformation. The crack growth rates in hydrogen-charged SUS304 and SUS316 were accelerated. The crack growth rate in hydrogen-charged SUS316L was slightly higher than uncharged SUS316L. However, the crack growth rate in SUS405 hardly changed in comparison with uncharged specimens. The matensitic transformation on fatigue fracture surface was detected by X-ray diffraction both in hydrogen-charged and uncharged specimens of SUS304, SUS316 and even in SUS316L. However, the fracture surface of SUS316L, in which the crack growth rate was increased slightly by hydrogen, showed less martensitic transformation than that of SUS304 or SUS316. It is presumed that martensitic transformation in the vicinty of fatigue crack tip contributed to the effect of hydrogen on crack growth rate. Fatigue tests of SUS304 and SUS316L, which were pre-strained at -70℃ to enhance a martensitic transformation, were carried out to study the influence of hydrogen and martensite on crack growth. Crack growth rate was remakably increased by hydroggen in not only pre-strained SUS304 but also in pre-strained SUS316L. The hydrogen content of pre-strained hydrogen-charged specimen was much higher than unstrained hydrogen-charged specimens due to the increase in martensite through which hydrogen diffuses much easier and faster than through austenite. The slip bands around crack tip in the hydrogen-charged specimens were less and more discrete than that in the uncharged specimens.