1 0 0 0 OA 年録

出版者
巻号頁・発行日
vol.[532],
著者
Austenfeld Jr.Robert B. Austenfeld Jr.Robert B.
雑誌
修道商学
巻号頁・発行日
vol.47, no.2, pp.55-108, 2007-02-28
出版者
巻号頁・発行日
vol.[1],
著者
今泉 宏之 南部 直樹 永井 恒司
出版者
The Pharmaceutical Society of Japan
雑誌
Chemical and Pharmaceutical Bulletin (ISSN:00092363)
巻号頁・発行日
vol.28, no.9, pp.2565-2569, 1980-09-25 (Released:2008-03-31)
参考文献数
13
被引用文献数
66 96

An X-ray diffraction method for determination of the degree of crystallinity of indomethacin was established, and the transition rate of indomethacin from amorphous to crystalline form was investigated. The transition of the amorphous form to crystalline form at 20°, 30°and 40°followed first-order kinetics and the Arrhenius plot showed good linearity. The amorphous form was shown to change to form I at 100% relative humidity (RH), to form I or II at 89% RH and to form I at 79% and 69% RH at 30°. The transition rate of the amorphous form to form II at 100% RH was larger than that at 89% RH. A good linear relation was observed between the maximum amount of water absorbed (log scale) and the degree of crystallinity at 100% or 89% RH at 30°. The dissolution rate of the amorphous form was higher than those of forms I and II. The amorphous form showed better tablet-forming properties than the crystalline form.
著者
阿部 仁美 櫻井 富士朗 Hitomi Abe Fujiro Sakurai 帝京科学大学生命環境学部アニマルサイエンス学科 帝京科学大学生命環境学部アニマルサイエンス学科 Teikyo University of Science Faculty of Life & Environmental Sciences-Department of Animal Science Teikyo University of Science Faculty of Life & Environmental Sciences-Department of Animal Science
出版者
帝京科学大学
雑誌
帝京科学大学紀要 = Bulletin of Teikyo University of Science (ISSN:18800580)
巻号頁・発行日
vol.10, pp.15-23, 2014-03-31

Budgerigars use contact calls and warble-songs. Previous studies have found that they acquire these songs through vocallearning, but to date, there have been no long term experimental studies of their vocalizations or social interactions. Thepurpose of this study was to establish a basic understanding of budgerigar vocal ethnology. We recorded all sounds made byfour budgerigars (male=4, female=3) kept in separate cages in a same experimental box for fixed periods (12-h light/darkcycle). There was great diurnal variation in vocalizations, but the variation decreased from lights up to off and during thelights-off period. The variation in vocalizations was also positively related to changes in humidity. The frequency of soundsproduced by the group of males was higher than that of the group of males and females mixed together. The response rate forcontact call varied among individuals which suggests that hierarchy existed in vocal communication. However, the hierarchychanged depending on the membership in a group.

1 0 0 0 OA 南巡盛典120卷

著者
清高晉等撰
巻号頁・発行日
vol.[20], 1771
著者
生塩 孝則 遠藤 寛二 山本 恵司
出版者
公益社団法人 日本薬学会
雑誌
YAKUGAKU ZASSHI (ISSN:00316903)
巻号頁・発行日
vol.116, no.11, pp.866-875, 1996-11-25 (Released:2008-05-30)
参考文献数
21
被引用文献数
3 4

The physicochemical properties of the enantiomer and racemates of suplatast tosilate (ST) were investigated by means of infrared spectroscopy, solid-state 13C CP/MAS NMR spectroscopy, thermal analysis, and X-ray diffraction analysis, and by measuring the solubility and hygroscopy. The infrared and NMR spectra and X-ray diffraction pattern of the enantiomer were distinctly different from those of the racemate. The melting point of the enantiomer was lower than that of the racemate by 5°C, while the solubility of the enantiomer was 1.3 times higher than that of the racemate. The hygroscopic rate of the enantiomer was greater than that of the racemate. These results suggested that ST was classified into a racemic compound crystal. Furthermore, by comparing the relative peak intensity ratios on X-ray diffraction patterns of crystals with various optical purities prepared by recrystallization, it was found that a mixture of racemic compound crystals and either of racemic mixture crystals or racemic solid solutions was obtained by recrystallization of ST in the content of 0 to 64%ee, while the recrystallization of ST in the content of more than 64%ee led to the formation of racemic mixture crystals or racemic solid solutions.
著者
多田 幸雄 山脇 一郎 上田 修一 松本 宏 松浦 直資 安本 三治 江田 昭英 堀 幹夫
出版者
Chem-Bio Informatics Society
雑誌
Chem-Bio Informatics Journal (ISSN:13476297)
巻号頁・発行日
vol.2, no.3, pp.86-94, 2002 (Released:2002-10-31)
参考文献数
10
被引用文献数
1 1

I 型アレルギー疾患治療薬を開発する目的でトシル酸 2-ヒドロキシエチルジメチルスルホニウム (1) 誘導体の抗アレルギー作用を検討した。それらの中でトシル酸 2-アルコキシと2-フェノキシエチルジメチルスルホニウムの数化合物がIgE 誘導ラット同種受身皮膚アナフィラキシー(PCA)の抑制作用を示した。抗アレルギー作用および急性毒性と化合物の疎水性または電子的性質(HOMOまたは酸素原子上の電荷)との間に相関が見られた。そしてトシル酸2-フェノキシエチルジメチルスルホニウム(5)を、次の開発段階における第二のリード化合物として選定した。
出版者
巻号頁・発行日
vol.[58] 廻船、屋形船持、堀浮芥定浚請負人 神田組・深川組,
著者
宇津木 成介
出版者
神戸大学
雑誌
国際文化学研究 : 神戸大学国際文化学部紀要 (ISSN:13405217)
巻号頁・発行日
vol.29, pp.73-91, 2007-12

How many basic emotions are? As William James suggested, we may have an endless list of words expressing emotional states if we enumerate them. In this article the author briefly introduced "seven (basic) emotions" which seem to be based on Buddhism. Charles Darwin provided 37 affective words in eight chapter titles in his "On the expression of the emotions in man and animals." To the contrary J.B. Watson argued he found only three basic emotions X,Y, and Z in his "Behaviorism." James listed seven names of emotions in his 1884 article, and eight names in his 1892 textbook. Only anger and fear appeared in the both lists. He thought that "the varieties of emotion are innumerable," so he seemed to try not to talk about each emotion but to explain emotion per se. Researchers like Wundt have suggested the dimensional structure of emotion. Later, Plutchik introduced his three dimensions theory of emotions and maintained that there are 8 primary emotions and they compose other emotions as three primary colors do. His dimensional view of emotions seems to be the opposite to the one that we humans have a set of basic instincts and each emotion connects to the instinct. James' view of emotion could be understood on a sort of physiological continuum, he also subscribed the idea that humans have discrete instincts. Watson, criticizing James, followed the way suggested by James, that emphasizes the stimulus arousing the emotional response. Although he did not deny the basic action parts observed in the newborn child, he did deny the importance of human instinct which was laid a great importance by McDougall. Woodworth showed that 58 emotional words could be classified into 11 classes. He also indicated that there might be six categories of emotions using Feleky's data. The six categories showed a similar circular structure proposed by Plutchik. In sum, most common number of basic emotions will be 6 to 8. The modern theories of basic emotions should be compared with the older philosophical views of emotions speculated by Tomas Aquinas, Descartes, and Spinoza who proposed 3 to 6 basic emotions that humans have.
著者
明祁承〓撰
巻号頁・発行日
vol.[5], 1000
著者
大村 英正
出版者
記録管理学会
雑誌
レコード・マネジメント (ISSN:09154787)
巻号頁・発行日
vol.48, pp.11-28, 2004

企業経営はしばしば困難に直面するが、そのような時にこそ、そして普段から歴史を学び歴史に学ぶことが大切であり、その方法論が適正でなければならない。本稿では、企業で経営史料の管理、活用並びに会社史の編纂を担当した若干の経験をふまえて、非現用の企業史料を中心に、その定義、収集、評価、保存・管理、活用さらにビジネスアーキビストの育成について、問題提起を含めて私見を述べる。収集では着眼点と収集対象を、評価では評価の主体と史料価値の多面性について、保存・管理では原秩序の維持と出所の原則の重要性について、活用では史料の広範な利用の実例と可能性を中心に論考する。ビジネスアーキビストの育成については資質面と育成の制度に触れる。総じて、公共財としての性格をも持つ個々の企業の私的財産である企業史料の取り扱いについて全体像を整理してみた。これらは概論であり基本の考え方であって企業史料管理マニュアルではない。